甲醇中9种大环内酯类混标
Reference Material
This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO 9001.
Product Name(产品名称) 9 Macrolide Antibiotic Mix in Methanol,100μg/mL(甲醇中9种大环内酯类混标)
Part Number(产品编号) 80761GA
Lot Number(产品批号) -
Expiry Date(失效日期) 2025-Dec-03________________________________________________
Storage(存储条件) (2-8)℃,Keep in the shade
(2~8)℃冷藏，置于阴凉处
(2~8)℃冷藏，置于阴凉处
Transportation(运输条件) Normal temperature transportation
(常温运输)
(常温运输)
| CERTIFIED | |||||
| Component No. (组分数) | Peak Sequence (出峰顺序) | Component (组分) | CAS No. | Concentration (μg/mL) (浓度) | Relative Expanded Uncertainty(%) (k=2) (相对扩展不确定度) |
| 1 | 1 | Lincomycin Hydrochloride1 (盐酸林可霉su) | 859-18-7 | 100(free base) | 3 |
| 2 | 2 | Spiramycin (螺旋mei素) | 8025-81-8 | 100 | 3 |
| 3 | 3 | Tilmicosin (替mi考星) | 108050-54-0 | 100 | 3 |
| 4 | 4 | Clindamycin Hydrochloride1 (盐酸克林mei素) | 21462-39-5 | 100(free base) | 3 |
| 5 | 5 | Oleandomycin Phosphate1 (磷酸竹tao霉素) | 7060-74-4 | 100(free base) | 3 |
| 6 | 6 | Erythromycin (红霉su) | 114-07-8 | 100 | 3 |
| 7 | 7 | Tylosin A tartrate1,2 (酒石酸泰洛星) | 74610-55-2 | 100(free base) | 3 |
| 8 | 8 | Leucomycins (吉他mei素) | 1392-21-8 | 100 | 3 |
| 9 | 9 | Josamycin (交沙mei素) | 16846-24-5 | 100 | 3 |
Instrument(检测仪器) HPLC/MS-MS
Column(色谱柱) C18(2.1x100mm,1.8μm)
Column Oven(柱温) 35℃
Method Details(方法参数)
A:0.1% Formic Acid(0.1% 甲酸)
B:Acetonitrile(乙腈)
A:0.1% Formic Acid(0.1% 甲酸)
B:Acetonitrile(乙腈)
| Time/min | A/% | B/% |
| 0.00 | 90 | 10 |
| 0.50 | 90 | 10 |
| 4.00 | 5 | 95 |
| 5.50 | 5 | 95 |
| 6.00 | 90 | 10 |
| 7.00 | 90 | 10 |
Note
上一篇 : 80363JA蜂蜜中大环内酯类药物残留量测定 下一篇 : 81863c标准品/甲醇中9种大环内酯类混标
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