乙腈中43种糖皮质激素类混标
注：81099GH(套标)由81096GH乙腈中43种糖皮质激素类混标+81097GH 乙腈中8种性激素混标+81098GH乙腈中11种激素类药物混标+91493GH乙腈中曲安xi龙
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Reference Material
This certificate is designed in accordance with ISO 17034 and ISO Guide 31. This reference material (RM) was designed,produced and verified in accordance with ISO/IEC 17025, ISO 17034 and a registered quality management system ISO 9001.
Product Name(产品名称) 43 Glucocorticoid Mix in Acetonitrile,100μg/mL(乙腈中43种糖皮质激素类混标)
Part Number(产品编号) 81096GH
Lot Number(产品批号) -
Expiry Date(失效日期) 2025-Feb-27____________________________________________________
Storage(存储条件) (-18±5)℃,Keep in the shade
冷冻(-18±5)℃,置于阴凉处
冷冻(-18±5)℃,置于阴凉处
| CERTIFIED | |||||
| Component No. (组分数) | Peak Sequence (出峰顺序) | Component (组分) | CAS No. | Concentration (μg/mL) (浓度) | Relative Expanded Uncertainty(%) (k=2) (相对扩展不确定度) |
| 1 | 1 | Prednisolone (泼尼song龙) | 50-24-8 | 100 | 3 |
| 2 | 2 | Isoflupredone (异氟泼ni松) | 338-95-4 | 100 | 3 |
| 3 | 3 | Prednisone (泼尼song) | 53-03-2 | 100 | 3 |
| 4 | 4 | Hydrocortisone (氢化可的song) | 50-23-7 | 100 | 3 |
| 5 | 5 | Cortisone (可的song) | 53-06-5 | 100 | 3 |
| 6 | 6 | Methylprednisolone (甲基强的song龙) | 83-43-2 | 100 | 3 |
| 7 | 7 | Betamethasone (倍他米song) | 378-44-9 | 100 | 3 |
| 8 | 8 | Flumethasone (氟米song) | 2135-17-3 | 100 | 3 |
| 9 | 9 | Beclometasone (倍氯米song) | 4419-39-0 | 100 | 3 |
| 10 | 10 | Methylprednisolone Acetate (甲基泼尼song龙醋酸酯) | 53-36-1 | 100 | 3 |
| 11 | Desonide (地索奈de) | 638-94-8 | 100 | 3 | |
| 12 | 11 | Flunisolide (氟尼缩song) | 3385-03-3 | 100 | 3 |
| 13 | 12 | Fluocinolone Acetonide (氟轻song) | 67-73-2 | 100 | 3 |
| 14 | 13 | Triamcinolone Diacetate (曲安xi龙双醋酸酯) | 67-78-7 | 100 | 3 |
| 15 | 14 | Prednisolone 21-acetate (醋酸泼尼song龙) | 52-21-1 | 100 | 3 |
| 16 | 15 | Fluorometholone (氟mi龙) | 426-13-1 | 100 | 3 |
| 17 | 16 | Fludrocortisone Acetate (醋酸氟氢可的song) | 514-36-3 | 100 | 3 |
| 18 | 17 | Deflazacort (地夫ke特) | 14484-47-0 | 100 | 3 |
| 19 | 18 | Prednisone Acetate (醋酸泼尼song) | 125-10-0 | 100 | 3 |
| 20 | 19 | Cortisone 21-acetate (醋酸可的song) | 50-04-4 | 100 | 3 |
| 21 | 20 | Betamethasone Acetate (醋酸倍他米song) | 987-24-6 | 100 | 3 |
| 22 | 21 | Budesonide (布di奈德) | 51333-22-3 | 100 | 3 |
| 23 | 22 | Hydrocortisone17-butyrate (丁酸氢化可的song) | 13609-67-1 | 100 | 3 |
| 24 | 23 | Fluorometholone 17-acetate (醋酸氟mi龙) | 3801-06-7 | 100 | 3 |
| 25 | 24 | Hydrocortisone 17-valerate (氢化可的song戊酸酯) | 57524-89-7 | 100 | 3 |
| 26 | 25 | Triamcinolone Acetonide Acetate (醋酸曲an奈德) | 3870-07-3 | 100 | 3 |
| 27 | 26 | Diflorasone Diacetate (二氟拉song双醋酸酯) | 33564-31-7 | 100 | 3 |
| 28 | Fluocinonide (醋酸氟轻song) | 356-12-7 | 100 | 3 | |
| 29 | 27 | Prednicarbate (泼尼ka酯) | 73771-04-7 | 100 | 3 |
| 30 | 28 | Loteprednol Etabonate (氯替泼nuo) | 82034-46-6 | 100 | 3 |
| 31 | 29 | Amcinonide (安西nai德) | 51022-69-6 | 100 | 3 |
| 32 | 30 | Halobetasol Propionate (卤贝他索丙suan酯) | 66852-54-8 | 100 | 3 |
| 33 | 31 | Alclometasone Dipropionate (阿氯米song双丙酸酯) | 66734-13-2 | 100 | 3 |
| 34 | 32 | Megestrol Acetate (醋酸jia地孕酮) | 595-33-5 | 100 | 3 |
| 35 | 33 | Fluticasone Propionate (氟替ka松丙酸酯) | 80474-14-2 | 100 | 3 |
| 36 | 34 | Chlormadinone Acetate (醋酸氯di孕酮) | 302-22-7 | 100 | 3 |
| 37 | Hydrocortisone 21-acetate (醋酸氢化可的song) | 50-03-3 | 100 | 3 | |
| 38 | 35 | Medroxyprogesterone 17-acetate (醋酸jia羟孕酮) | 71-58-9 | 100 | 3 |
| 39 | 36 | Betamethasone Dipropionate (倍他米song二丙酸酯) | 5593-20-4 | 100 | 3 |
| 40 | 37 | Beclomethasone Dipropionate (倍氯米song双丙酸酯) | 5534-09-8 | 100 | 3 |
| 41 | Mometasone Furoate (糠酸莫美他song) | 83919-23-7 | 100 | 3 | |
| 42 | 38 | Diflucortolone Valerate (戊酸双氟可long) | 59198-70-8 | 100 | 3 |
| 43 | 39 | Clobetasone Butyrate (氯倍他song丁酸酯) | 25122-57-0 | 100 | 3 |
HPLC-MS/MS
Column(色谱柱) C18(2.1x50mm,1.8μm)
Column Oven(柱温) 35℃
Method Details(方法参数)
A: 0.1%Formic Acid(0.1%甲酸)
B: Acetonitrile(乙腈)
A: 0.1%Formic Acid(0.1%甲酸)
B: Acetonitrile(乙腈)
| Time/min | A/% | B/% |
| 0.00 | 90 | 10 |
| 2.00 | 90 | 10 |
| 5.00 | 50 | 50 |
| 7.00 | 50 | 50 |
| 10.00 | 40 | 60 |
| 14.00 | 40 | 60 |
| 14.10 | 90 | 10 |
| 18.00 | 90 | 10 |
Intended Use
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